離子束研磨拋光系統
儀器名稱 (Facility name)
離子束研磨拋光系統
Triple ion-beam milling system
規格與功能(Specifications and functions)
- 型號 (Model):Leica EM TIC 3X
- 離子源 (Ion sources):三支單體可獨立控制式離子槍 (Three independently controlled ion guns)
- 離子源功率(Ion beam power): 1 to 10 keV。
- 離子源電流(Ion beam current): 0.5 to 4.5 mA
- 離子束直徑 (FWHM of ion beam): 0.8 to 2.5 mm
- 橫截面研磨速率 (Cross sectional milling rate): average rate of 300 μm/hour @ 10 KeV for Si
- 最大樣品尺寸(橫截面) (Maxium size of cross section samples):40 mm x 40 mm x 10 mm (t)
- 研磨範圍(橫截面) (Milling range of cross section samples):1 mm in depth (max.) and 4 mm in width (max.)
- 最大樣品尺寸(平面拋光) (Maxium size of planer samples):35 mm in diameter/10mm in height
- 研磨範圍(平面拋光) (Milling range of planer samples):25 mm in diameter (max.)
- 使用氣體 (gas): Ar (99.999 % purity)
- 真空系統(Vacuum system):Oil-free, <1x10-5 mbar
使用規定與注意事項 (Rules and notices)
- 進行橫截面離子切割與拋光之試片表面需用大於1,000號之砂紙將試片表面磨平。
Cross-sectional samples have to be ground by SiC grinding paper (#1000) to a flat surface prior to ion milling.
- 進行平面拋光之試片表面先需用標準機械研磨拋光(mechanical polishing)方式完成表面拋光。
Samples have to be polished mechanically by SiC grinding papers and Al2O3 powders according to the standard metallographic procedures prior to planar milling.
- 離子切割與拋光過程試片溫度可能上升,最高溫度通常低於70oC。
Sample temperature may raise to as high as 70 oC during ion bombardment.
收費標準(Service charge)
委託操作(廠商) (Operator service (Non-academic organization))
(1) 橫截面試片離子切割 (cross sectional milling)
2 hrs or below : 1000 NTD/piece
2-3 hrs : 1,250 NTD/piece
3-4 hrs : 1,500 NTD/piece
4-6 hrs : 2,000 NTD/piece
- 平面拋光(planar milling): 1,000 NTD/piece
委託操作(外校) (Operator service (Academic organization))
(1) 橫截面試片離子切割 (cross sectional milling)
2 hrs or below : 800 NTD/piece
2-3 hrs : 1,000 NTD/piece
3-4 hrs : 1,200 NTD/piece
4-6 hrs : 1,600 NTD/piece
- 平面拋光(planar milling): 800 NTD/piece
委託操作(本校) (Operator service (NSYSU))
(1) 橫截面試片離子切割 (cross sectional milling)
2 hrs or below : 600 NTD/piece
2-3 hrs : 750 NTD/piece
3-4 hrs : 900 NTD/piece
4-6 hrs : 1,200 NTD/piece
(2)平面拋光(planar milling): 600 NTD/piece
自行操作(本系) (Self-operation)
(1) 橫截面試片離子切割 (cross sectional milling)
2 hrs or below : 500 NTD/piece
2-3 hrs : 600 NTD/piece
3-4 hrs : 750 NTD/piece
4-6 hrs : 1,000 NTD/piece
(2)平面拋光(planar milling): 500 NTD/piece
聯絡方式 (Contact information)
儀器指導教授 (Professor in-charge):張六文教授 (Professor Liuwen Chang)
操作人員與聯絡人 (Operator):顏采蓉 (Ms Yen)/ 楊國裕 (Mr. K-Y Yang)
聯絡電話(Tel):07-5252000 #4085/07-5252000 #4087
電子信箱(e-mail):judyyen123@staff.nsysu.edu.tw/ kuoyu@mail.nsysu.edu.tw
儀器地點(Location):材料大樓三樓3021室 (Room工MS3021)
開放時間 (Opening hours)
週一至週五 早上8:30至下午5:30
8:30 AM – 5:30 PM, Monday through Friday